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By Patrizio G., Tomassini A.

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Additional info for A Characterization of Affine Hyperquadrics

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4. 5. 6. 7. 8. 9. 10. 11. 12. 13. 14. 15. 16. 17. 18. 19. 20. 21. 22. 23. 24. 25. 26. 27. 28. 29. 30. 31. 32. 33. 34. 35. 36. 37. 38. Slater JC (1941) J Chem Phys 9:16 Blinc R (1960) J Phys Chem Solids 13:204 Blinc R, Svetina S (1966) Phys Rev 147:423–430 Wul B, Goldman IM (1945) C R Acad Sci URSS 46:139 Wul B, Goldman IM (1946) C R Acad Sci URSS 51:21 Matthoas BT (1949) Phys Rev 75:1771 Matthias BT, Remeika JP (1956) Phys Rev 103:262, 76:1886 Shirane G, Hoshino S, Suzuki K (1950) Phys Rev 80:1150 Slater JC (1950) Phys Rev 78:748 Cochran W (1960) Adv Phys 9:387 Anderson PW (1960) In: Skanavi GI (ed) Fizika Dielektrikov.

At T > TN , they merge to a narrow doublet with a separation of about 10 ppm. As for to the 13 C data, the 17 O data were analyzed by plotting the average of the four peaks as a function of temperature. Figure 12 shows the corresponding plot. An important observation was that the position of the coalesced peak (doublet) did not coincide with the average of the four low-temperature peaks; this point is discussed in detail in the following section. The doubling was not related to any crystal effects, because measurements with powders exhibited a similar splitting [26].

A detailed analysis suggested that the 15 N NMR study of the ADA and ADP lattices, which undergo a transition at 216 and 148 K, might offer the best combination in terms of available MAS techniques at the feasible temperatures, leading to the following results. 1 15 N NMR in NH H AsO 4 2 4 Figure 17 shows a comparison between 15 N signals from CP-MAS spectra of an ADA crystal, without any spinning (Fig. 17a) and with spinning (Fig. 17b) at 5 kHz. The line width decreases from 80 Hz to only about 12 Hz under spinning, again demonstrating the significant resolution enhancement provided 44 O.

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A Characterization of Affine Hyperquadrics by Patrizio G., Tomassini A.


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